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The instrument

Spectrally X1 INLINE - built for the silicone line.

A process Raman analyzer for continuous composition and cure measurement inline - read directly in the reactor or line rather than pulled to a lab - 24/7, with no sampling and no consumables.

01 The instrument

A process Raman analyzer built for the line.

Spectrally X1 INLINE reads siloxane composition and cure state directly in the reactor or line - 24/7, without sampling and without consumables. The spectrum is acquired in the process, the result arrives in under 5 seconds, and the value streams to your PLC or DCS continuously.

Spectrally X1 INLINE - the complete analyzer cabinet
Catalog specification

Two excitation wavelengths are available - 785 nm and 1064 nm, the latter for strongly fluorescing media - at 600 mW and 800 mW respectively, limited to 30 mW for ATEX applications. Detection is a back-thinned, TEC-cooled CCD with a proprietary TEC controller.

Measurement principleRaman spectroscopy
Laser wavelength785 nm / 1064 nm
Laser power600 mW @ 785 nm; 800 mW @ 1064 nm; 30 mW for ATEX applications
Spectral range300-1650 cm⁻¹ or 300-3500 cm⁻¹
Spectral resolution8 cm⁻¹
Acquisition time5-300 s
DetectorBack-thinned CCD, TEC-cooled
Measurement channelsUp to 2 (expandable on request)
Fiber optic reachUp to 100 m
CommunicationPROFIBUS, PROFINET, GSM
CalibrationAutomatic - reference integrated in the probe
Laser lifetimeMin. 2 years
HMITouchscreen (SpectrallyUI)
SoftwareSpectrally OS on Debian GNU/Linux 13.2
ProbeSpectrally X1 PROBE - IP67, ATEX / IECEx Zone 0, self-cleaning; fused silica or sapphire (Al₂O₃) window

Values per the Spectrally Raman Analyzers product catalog, 2026-05.

02 Spectrally X1 PROBE

The part of the system that lives in your process.

An immersion Raman probe for direct in-situ analysis in the reactor or line - no sampling, no conditioning loop. Rated to 16 bar and +125 °C, pH 2-10 in continuous service and 1-14 short-term, with IP67 ingress protection and an ATEX / IECEx Zone 0 rating. Fused silica is the standard window; a sapphire (Al₂O₃) window handles the corrosive HCl of a chlorosilane stream.

Spectrally X1 PROBE flange with labels on a process line
Probe specification

The probe measures in reactors, pipelines and process tanks, in batch and continuous operation. It handles liquid silicones, fluids and slurries - from PDMS condensation through LSR/HCR cure and the chlorosilane line.

Probe typeImmersion, dual fiber-optic connection
Laser wavelength785 nm / 1064 nm
Process pressureUp to 16 bar
Process temperature-40 to +125 °C
Process pH2-10 continuous; 1-14 short-term
Ingress protectionIP67
Hazardous areasATEX / IECEx Zone 0
Housing316L stainless steel; POM-C / POM-C ESD (ATEX version)
Optical windowFused silica standard; sapphire (Al₂O₃) for corrosive chlorosilane / HCl media
MountingFlange, Tri-Clamp, retractable process holder
CleaningSelf-cleaning module - automatic retract-rinse-return cycle
Self-cleaning probe cycle
Retract
Rinse
Return
Curing silicone films optical windows. The retractable self-cleaning module cycles retract → rinse → return automatically, keeping the window clean in filming media without interrupting continuous measurement.

Dual fiber-optic connection

Separate excitation and collection fibers simplify installation and keep the signal stable. The probe connects to the analyzer over a fiber-optic cable - up to 100 m of reach.

Immersion install, no bypass

Mounts directly in the reactor, pipeline or tank via flange, Tri-Clamp or retractable process holder. No sample extraction, no conditioning loop between the silicone and the measurement.

Window and area matched to the medium

Fused silica is standard; a sapphire (Al₂O₃) window handles the corrosive HCl by-product of a chlorosilane stream. ATEX / IECEx Zone 0, with laser power limited to 30 mW for ATEX applications.

Fiber optic reach
0m

Probe at the process, analyzer cabinet up to 100 m away.

Probe pressure rating
0bar

Process rating of the immersion X1 PROBE, up to +125 °C.

Spectral resolution
0cm⁻¹

Across a 300-1650 or 300-3500 cm⁻¹ spectral range.

Measurement channels
0

Two measurement points per analyzer, expandable on request.

03 Spectrally OS

From raw spectrum to an operational answer.

Spectrally OS is the analytical layer of the platform. It translates spectra into concentrations, ratios and cure state, flags deviations, raises alarms and writes the quality record - locally, on the analyzer.

Spectrally X1 INLINE on a mobile stand with a flow cell
Model stack

The analytical work runs on AI / advanced chemometrics with a CNN core - deep pattern recognition across the diagnostic silicone bands: Si-H ~2160 cm⁻¹, vinyl C=C ~1600 cm⁻¹ and the cyclic/linear siloxane band ~490 cm⁻¹. Classical PLS and PCA are carried as the benchmark this core is measured against.

Supported instrumentsSpectrally X1 LAB / X1 PORTABLE / X1 INLINE
Predictive modelsAI / advanced chemometrics, CNN core (PLS / PCA benchmark)
Spectral databaseProprietary + public, ~28,000 spectra
Operator interfaceSpectrallyUI, touchscreen
Operating systemDebian GNU/Linux 13.2
CalibrationAutomatic, based on the reference signal readout
Data exportCSV / PDF / RAW
User managementRole-based access control (RBAC)
Data storageLocal database
Industrial protocolsPROFIBUS / PROFINET / GSM

Deviation flags, not just numbers

Cure PASS/FAIL classification, anomaly detection and batch-conformity checks against specification. Alarms and quality reports are written for plant operators, not spectroscopists.

A model lifecycle, not a black box

Calibration, validation, maintenance. A model starts in feasibility on your silicone matrix, is refined on production data, and re-calibrated when a grade or recipe changes. Every model change is logged and auditable.

No line stop for updates

Model updates deploy without stopping the analyzer or the line. Measurement and local logging keep running if the network drops - data lives in the local database.

Spectrally product family - X1 LAB, X1 PORTABLE, X1 INLINE and the X1 PROBE

One software layer across the Spectrally family. Models built during feasibility on Spectrally X1 LAB migrate to Spectrally X1 INLINE in production - the same analytics, moved from the lab bench to the silicone line.

04 Raman vs alternatives

What changes against GC/MS, gel-time, DSC and NIR.

The differences are physical, not promotional. These are the factual points that matter for a silicone stream - and how the lab methods and inline Raman divide the work.

Alternative technique
Inline Raman - Spectrally X1 INLINE
×GC/MS: 60-120 min per sample for residual cyclics, with sampling and extraction
Cyclic-vs-linear read from the ~490 cm⁻¹ siloxane band in-process, no sampling
×Gel-time and DSC: cure state offline - observational, or a 30-90 min run
Crosslinking confirmed live from the vanishing Si-H ~2160 cm⁻¹ and vinyl C=C ~1600 cm⁻¹ bands
×Inline viscometry: a molecular-weight proxy, but no composition
Chain length and composition read directly from the spectrum, not inferred
×NIR: does not separate cyclic from linear, limited selectivity with HCl present
Specific siloxane bands resolve cyclic from linear; a sapphire window handles chlorosilane HCl

A clean division of labor

ICP
Residual platinum catalyst
The Karstedt Pt residual is certified by ICP as an element. Raman owns the composition and crosslinking side of the batch record; ICP owns the trace-metal number.
GC/MS · DSC
The accredited reference methods
GC/MS and DSC stay the reference. Inline Raman runs continuously in-process, so the offline methods become scheduled verification rather than the bottleneck.

Inline Raman moves the composition and cure measurement into the process, in seconds, where decision time and continuity decide the batch. The lab methods keep doing what they do best - verifying against a continuous, time-stamped inline record.

05 Installation & service

The installation, in practical terms.

What the analyzer needs from your plant, and what it does not.

Fiber optic reach
Up to 100 m

The probe sits at the process. The analyzer cabinet can sit up to 100 m away, connected by fiber.

Measurement channels
Up to 2 standard

One analyzer serves two measurement points. More channels available on request.

Calibration
Automatic

Runs against a reference integrated in the probe - no manual recalibration routine.

Warm-up
30 min

From power-on to measurement. Continuous 24/7 operation after that.

Spectrally X1 PROBE flange before installation

Utilities

230 V AC, 50/60 Hz, 300 W power draw. Operating environment 0-45 °C and 20-70% RH, non-condensing.

Process connections

Flange, Tri-Clamp or retractable process holder, matched to the reactor or line. A sapphire window is specified where a chlorosilane stream carries corrosive HCl. Custom designs on request.

No consumables

No reagents and no consumables in routine operation. Rated laser lifetime is a minimum of 2 years.

Service and model upkeep

Installation and service are performed by authorized Gekko Photonics technicians. Model maintenance runs through Spectrally OS - validation, re-calibration when a grade or recipe changes, deployed without stopping the line.

Your next step

Put the analyzer through your silicone first.

Send representative samples or R&D data from your PDMS, LSR/HCR, chlorosilane or medical-grade silicone process. We build and validate a chemometric model on your silicone matrix in the Gekko lab and report exactly what Spectrally X1 INLINE reads on your line - before any hardware decision.

What would you like to do?

Explore Spectrally X1 INLINE ->